First things first, we are going to bring an Erlenmeyer flask of water to 212°F. Yes, we are going to boil it with heat. This is is going to help us drop the pressure, and we will get to the cool ...

Mix 175g of NaOAc trihydrate with 50mL distilled water in a very clean 500mL erlenmeyer flask and heat in a boiling water bath until all solid is dissolved. Remove from bath, ... Carefully drop a seed ...

Following this, the flask is connected to a reflux condenser for refluxing at 120 °C, for 15 ± 1 minute. In the next step, the Erlenmeyer flask and condenser are taken off the heating plate so that ...

When an Erlenmeyer flask is used, it proved to be simpler to wrap the tubing directly into flask. ... Heat the US bath to 25 °C. The temperature should be constant at 25 °C. 39.