Integrating Spinsolve NMR in labs supports green chemistry, reducing environmental impact while enhancing students' practical ...

Figure 3 shows the 1 H/ 13 C NMR spectra of methanol intermediates of the reaction system containing Pd/TiO 2, D 2 O and CH 3 OH. In this system, CH 3 OD would be generated because of the fast H/D ...

Figure 1. 1 H NMR spectrum of 3-buten-1-ol in protonated methanol. Relative concentration of the solute is higher than a typical NMR sample for clarity, but this ratio is not uncommon in an actual ...

A small methanol sample is recrystallized, and the blue-grey needles are filtered using Buchner filtration, washed with cold methanol, and dried in a vacuum desiccator. With the help of the ...